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Accessories for CHROMABOND®

Description

Properties
Description: Glass fiber frits for glass columns, 6 ml
Manufacturer Article Number: 730192
UNSPSC: 41-10-49-22
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Accessories

Macherey-Nagel GmbH & Co. KG

Macherey-Nagel GmbH & Co. KG
Adapters for CHROMABOND® glass columns
From CHF 402.40*
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Extraction kits Copure® QuEChERS
Extraction and clean-up mixtures for sample preparation in the pesticide analysis of vegetable foodstuffs according to EN 15662 using GC/MS or LC/MS after acetonitrile extraction and purification using the dispersive SPE-QuEChERS method.The samples are first extracted with Mix A. Purification is done with one of the following mixtures:Mix B (Clean-up mixture for fruits and vegetables with low fat content, e.g. apples, strawberries)Mix C (Clean-up mixture for fruits and vegetables with high fat content, containing oil/wax, e.g. avocados)Mix D (Clean-up mixture for moderately chlorophyll/carotenoid-containing fruits and vegetables, e.g. carrots, salad)Mix E (Clean-up mixture for fruits and vegetables with high chlorophyll/carotenoid content, e.g. sweet peppers, spinach)If required, add ceramic homogenising beads for better mixing.Mix A contains a bag with the required amount of mixture and a 50 ml empty tubeMix B, C, D and E are pre-weighed into a 15 ml tube
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CHROMABOND® C18
Octadecyl modified silica phase for SPE, not endcappedBase material silica, pore size 60 Å, particle size 45 µm for C18, specific surface 500 m²/g, pH stability 2 to 8 octadecyl phases, not endcapped, carbon content 14 % possesses more free silanols (SiOH), which allow secondary interactions with polar groups of the analytes.Recommended applications: non-polar compounds, pesticides.
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CHROMABOND® C18 ec
Octadecyl modified silica phase for SPE, endcappedBase material silica, particle size 45 µm for C18 ec, specific surface 500 m²/g, pH stability 2 to 8. Octadecyl phases, endcapped, carbon content 14 % very non-polar, hydrophobic interactions with a wide variety of organic compounds. Advantageous for clean-up of samples with large structural variations (polarity differences).Recommended applications: non-polar compounds, aflatoxins, amphetamines, antibiotics, antiepileptics, barbiturates, caffeine, drugs, preservatives, fatty acids, nicotine, PAHs, pesticides, PCBs, heavy metals, vitamins. Very well suited for desalting of samples.
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CHROMABOND® C18 ec, glass column
Octadecyl modified silica phase for SPE, endcappedBase material silica, particle size 45 µm for C18 ec, specific surface 500 m²/g, pH stability 2 to 8. Octadecyl phases, endcapped, carbon content 14 %, very non-polar, hydrophobic interactions with a wide variety of organic compounds. Advantageous for clean-up of samples with large structural variations (polarity differences).Recommended applications: non-polar compounds, aflatoxins, amphetamines, antibiotics, antiepileptics, barbiturates, caffeine, drugs, preservatives, fatty acids, nicotine, PAHs, pesticides, PCBs, heavy metals, vitamins. Very well suited for desalting of samples.
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CHROMABOND® C8
Octyl modified silica phase for SPE, not endcappedBase material silica, pore size 60Å, particle size 45µm, specific surface 500m²/g, pH stability 2 to 8. Octyl phase, not endcapped, carbon content 8%, similar to C18, however slightly more polar. Secondary interactions with polar compounds are more pronounced due to shorter alkyl chains.Recommended applications: pesticides, PCBs.
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CHROMABOND® C18 Hydra
Octadecyl modified silica phase for SPE of polar analytesBase material silica, pore size 60 Å, particle size 45 µm, specific surface 500 m²/g, pH stability 2 to 8, special octadecyl phase for polar analytes, not endcapped, carbon content 15 %.Recommended applications: more polar compounds like pesticides and their polar degradation products, phenols, phenoxycarboxylic acids, nitroaromatics, pharmaceuticals.
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CHROMABOND® Easy
Polar modified polystyrene-divinylbenzene copolymer with a weak anion exchangerSpecific surface 650 to 700 m²/g, particle size 80µm, pore size 50 Å, pH stability 1 to 14. Due to bifunctional modification much more hydrophilic than conventional polystyrene-divinylbenzene polymers and thus easily wettable with water.Recommended applications: polar herbicides / pesticides from water (acidic, neutral, basic), polar phenols from water, polyaromatic compounds, polychlorinated biphenyls, drug analysis from urine, blood, serum, plasma pharmaceuticals / active ingredients from tablets, creams.Due to the bifunctional modification CHROMABOND® Easy is considerably more hydrophilic than conventional polystyrene-divinylbenzene polymers and thus easily wettable with water. The Easy effect: Aqueous samples can be loaded directly without preconditioning! This means that little or even no conditioning is needed, in contrast to standard SPE materials, where recovery rates normally decrease, in the worst case down to zero! Depending on the separation task conditioning may be required and is recommended for method development. A positive side effect of the excellent wettability: there is no decrease of recovery rates, if the cartridge runs dry, therefore automation is easier or, in some cases compared to silica materials, only feasible with CHROMABOND® Easy, because a permanent vacuum can be used without supervision.Further advantages of using a polymeric material:high surface, this means very high binding capacity (2 - 5 times higher than silica-based adsorbents)less adsorbent is needed in the cartridge (without losing sensitivity or recovery)faster analysis, because the height of the adsorbent bed can be reducedacidic or basic solvents (e. g. TFA) do not destroy the phase, or lead to unintended side productsBecause of the polar modification the material is suitable for a broad range of compounds (acidic, neutral, basic, polar and nonpolar substances). Highly reproducible recovery rates can be obtained, even if the cartridge runs dry (especially advantageous when using 96-well plates, where stopcocks are not available!)
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