Skip to main content Skip to search Skip to main navigation
Menu

QuEChERS adsorbent CHROMABOND® Diamino / PSA

Description
QuEChERS method and pre-mixes
Within a few years after its devleopment by Anastassiades et al. the QuEChERS method has gained a leading position for determination of pesticide residues in food by GC-MS or LC-MS allowing rapid and cheap clean-up of strong matrix-contaminated samples.
Standard clean-up of food samples
10 g sample are homogenised with 10 ml acetonitrile. After adding the internal standard the sample is shaken with 4 g MgSO4 and 1 g NaCI and afterwards centrifuged. 1 ml of the supernantant is spiked with 25 mg CHROMABOND® Diamino and 150 mg MgSO4 and shaken again. After centrifugation the supernatant is injected into the GC/MS.

Special silica phase for determination of pesticides in food samples with primary and secondary amine functions (PSA).
Particle size 45 µm, specific surface 500 m2/g, pH-stability from pH 2 to 8.

Properties
Manufacturer Article Number: 730653
Weight: 100 g
Skip product gallery

Similar products

CHROMABOND® vacuum manifolds and accessories
For simultaneous preparation of up to 12 or 24 samples, replacement parts and accessories for special applications.Vacuum manifold complete consists of: glass cabinet with lid and lid gasket, removable needles on lower side of lid, vacuum gauge, control valve, valves and caps, variable rack.
From CHF 57.40*

Extraction kits Copure® QuEChERS
Extraction and clean-up mixtures for sample preparation in the pesticide analysis of vegetable foodstuffs according to EN 15662 using GC/MS or LC/MS after acetonitrile extraction and purification using the dispersive SPE-QuEChERS method.The samples are first extracted with Mix A. Purification is done with one of the following mixtures:Mix B (Clean-up mixture for fruits and vegetables with low fat content, e.g. apples, strawberries)Mix C (Clean-up mixture for fruits and vegetables with high fat content, containing oil/wax, e.g. avocados)Mix D (Clean-up mixture for moderately chlorophyll/carotenoid-containing fruits and vegetables, e.g. carrots, salad)Mix E (Clean-up mixture for fruits and vegetables with high chlorophyll/carotenoid content, e.g. sweet peppers, spinach)If required, add ceramic homogenising beads for better mixing.Mix A contains a bag with the required amount of mixture and a 50 ml empty tubeMix B, C, D and E are pre-weighed into a 15 ml tube
From CHF 65.00*

CHROMABOND® XTR
Kieselguhr phase for liquid-liquid extractionBase material coarse-grained kieselguhr, large pore size, high pore volume, constantly high batch-to-batch quality, pH working range 1 to 13.Application: liquid-liquid extraction of highly viscous aqueous solutions such as physiological fluids (blood, plasma, and serum) in clinical chemistry, dyes in textiles, environmental and food analysis.Glass columns availlable on request.
From CHF 123.10*

CHROMABOND® OH (Diol)
Diol modified silica phase for SPEBase material silica, pore size 60Å, particle size 45µm, specific surface 500m²/g, pH stability 2 to 8, diol phase, carbon content 5.5%, polar properties similar to SiOH.Recommended application: antibiotics, prostaglandins.
From CHF 197.60*

CHROMABOND® C6H5
Phenyl modified silica phase for SPEBase material silica, pore size 60Å, particle size 45µm, specific surface 500m²/g, pH stability 2 to 8. Phenyl phase, carbon content 8%polarity similar to C8. In addition to hydrophobic interactions more selective adsorption is possible by Π-Π interactions due to the electron density of the phenyl ring.Recommended applications: aflatoxins, caffeine, phenols.
From CHF 226.80*

CHROMABOND® NH2
Aminopropyl modified silica phase for SPEBase material silica, pore size 60Å, particle size 45µm, specific surface 500m²/g, pH stability 2 to 8, aminopropyl phase, carbon content 3.5%, polar, weak anion exchanger.Recommended applications: trace elements, lipids.
From CHF 197.60*

CHROMABOND® NAN
Special phase for SPE analysis of PCB from sludgeSpecial combination phase:N: sodium sulphate for removal of trace water.A: SiOH/AgNO3 phase for removal of sulphur, sulphur-containing and polar compounds.Recommended application: extraction of PCB from sludge.
From CHF 501.80*

CHROMABOND® C18
Octadecyl modified silica phase for SPE, not endcappedBase material silica, pore size 60 Å, particle size 45 µm for C18, specific surface 500 m²/g, pH stability 2 to 8 octadecyl phases, not endcapped, carbon content 14 % possesses more free silanols (SiOH), which allow secondary interactions with polar groups of the analytes.Recommended applications: non-polar compounds, pesticides.
From CHF 153.80*

CHROMABOND® HR-X
Spherical, hydrophobic polystyrene-divinylbenzene resin for SPEHydrophobic polystyrene-divinylbenzene copolymer pH stability 1 to14. High-purity material with highest reproducibility and lowest blank values due to a novel manufacturing process, spherical particles 85mm; pore size 55 to 60Å. Very high surface 1000m²/g; capacity 390mg/g (caffeine in water). Excellent recovery rates especially for the enrichment of pharmaceuticals/active ingredients due to the spherical structure of the particles, very homogeneous surface, and optimised pore structure.Recommended applications: pharmaceuticals/active ingredients from tablets, creams and water/waste water, drugs and pharmaceuticals from urine, blood, serum and plasma trace analysis of pesticides.Cartridges in further sizes and phases of the HR-X poduct range available on request.
From CHF 95.60*